2-(4-Bromophenyl)-N-(3-chloro-4-fluorophenyl)acetamide

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2-Chloro-N-(4-chloro-3-iodo­phen­yl)-4-(methyl­sulfon­yl)benzamide

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2-(4-Bromo­phen­yl)-N-(3-chloro-4-fluoro­phen­yl)acetamide

In the title compound, C(14)H(10)BrClFNO, the benzene rings form a dihedral angle of 64.0 (2)°. In the crystal, mol-ecules are linked via inter-molecular N-H⋯O, C-H⋯O, C-H⋯Cl and C-H⋯F hydrogen bonds into layers parallel to (001). The crystal was refined as a merohedral twin with a 0.935 (114):0.065 (14) domain ratio.

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In the crystal of the title compound, C(10)H(12)BrNO, inversion dimers linked by pairs of N-H⋯O hydrogen bonds generate R(2) (2)(8) loops. Further N-H⋯O hydrogen bonds link the dimers into sheets propagating in (100).

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4-Chloro-N-(4-chloro­phen­yl)-2-methyl­benzene­sulfonamide

In the title compound, C(13)H(11)Cl(2)NO(2)S, the conformations of the N-C bonds in the C-SO(2)-NH-C segment have gauche torsions with respect to the S=O bonds. Further, the conformation of the N-H bond is syn to the ortho-methyl group in the sulfonyl benzene ring. The torsion angle of the C-SO(2)-NH-C segment in the mol-ecule is 55.0 (2)°. The two benzene rings are tilted relative to each othe...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2012

ISSN: 1600-5368

DOI: 10.1107/s1600536812032977